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Residual Solvents Class 2 — Mix A on Rxi-624Sil MS (G43) by USP

Column | Rxi-624Sil MS, 30 m, 0.32 mm ID, 1.80 µm (cat.# 13870) |
Sample | Residual solvents Class 2 — Mix A (2013 Rev) (cat.# 36012) |
Diluent: | Water |
Injection | |
Inj. Vol.: | 1000 µL headspace-loop split (split ratio 5:1) |
Liner: | Premium 1.0 mm ID straight inlet liner (cat.# 23333.1) |
Headspace-Loop | |
Inj. Port Temp.: | 140 °C |
Instrument: | Tekmar HT-3 |
Inj. Time: | 1.0 min |
Transfer Line Temp.: | 105 °C |
Valve Oven Temp.: | 105 °C |
Needle Temp.: | 85 °C |
Sample Temp.: | 80 °C |
Sample Equil. Time: | 60 min |
Mixer time: | 5.0 min |
Mixing level: | 5 |
Mixer stabilize time: | 0.50 min |
Vial Pressure: | 10 psi |
Pressurize Time: | 5.0 min |
Pressure Equilibration Time: | 0.20 min |
Loop Pressure: | 5.0 psi |
Loop Fill Time: | 2.0 min |
Oven | |
Oven Temp.: | 40 °C (hold 20 min) to 240 °C at 10 °C/min (hold 20 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 2.2 mL/min |
Detector | FID @ 250 °C |
Make-up Gas Flow Rate: | 45 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 450 mL/min |
Data Rate: | 20 Hz |
Instrument | Agilent/HP6890 GC |
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