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Rapeseed FAMEs in Biodiesel Oils on Stabilwax
| Peaks | ||
|---|---|---|
| 1. | Myristic acid methyl ester | C14:0 |
| 2. | Palmitic acid methyl ester | C16:0 |
| 3. | Palmitoleic acid methyl ester | C16:1 |
| 4. | Stearic acid methyl ester | C18:0 |
| 5. | Oleic acid methyl ester | C18:1 |
| 6. | Linoleic acid methyl ester | C18:2 |
| Peaks | ||
|---|---|---|
| 7. | Linolenic acid methyl ester | C18:3 |
| 8. | Arachidic acid methyl ester | C20:0 |
| 9. | Gadoleic acid methyl ester | C20:1 |
| 10. | Behenic acid methyl ester | C22:0 |
| 11. | Erucic acid methyl ester | C22:1 |
| 12. | Lignoceric acid methyl ester | C24:0 |
| 13. | Methyl nervonate | C24:1 |
IS Methyl heptadecanoate
GC_PC00917
| Column | Stabilwax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624) |
| Sample | Rapeseed source of biodiesel (B100), prepared according to European Method EN 14103 |
| Injection | |
| Inj. Vol.: | 1.0 µL split (split ratio 100:1) |
| Liner: | Cyclosplitter (cat.# 20706) |
| Inj. Temp.: | 250 °C |
| Oven | |
| Oven Temp.: | 210 °C (hold 5 min) to 230 °C at 20 °C/min (hold 5 min) |
| Carrier Gas | H2, constant flow |
| Flow Rate: | 3 mL/min |
| Linear Velocity: | 60 cm/sec |
| Detector | FID @ 250 °C |
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