Innovative Chromatography Products
www.restek.it
www.restek.it
Questo cromatogramma potrebbe contenere analiti che sono sinonimi dei vostri parametri di ricerca.
Carfentrazone Ethyl in Dandelion Root Powder (Dietary Supplement) on Rxi-5Sil MS
GC_FF1172
| Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
| Sample | dandelion root powder spiked with 46 pesticides |
| QuEChERS Internal Standard Mix for GC/MS Analysis (cat.# 33267) | |
| anthracene for quality control (cat.# 33264) | |
| Diluent: | toluene |
| Conc.: | 80 pg/µL |
| Injection | |
| Inj. Vol.: | 1 µL splitless (hold 1.5 min) |
| Liner: | 5mm Splitless with wool (cat.# 22975-200.1) |
| Inj. Temp.: | 250 °C |
| Oven | |
| Oven Temp.: | 90 °C (hold 1.5 min) to 340 °C at 8 °C/min |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1.5 mL/min |
| Detector | MS |
| Mode: | |
| Analyzer Type: | TOF |
| Source Temp.: | 225 °C |
| Electron Energy: | 70 eV |
| Ionization Mode: | EI |
| Acquisition Range: | 45-550 amu |
| Spectral Acquisition Rate: | 5 spectra/sec. |
| Instrument | LECO Pegasus 4D GCxGC-TOFMS |
| Notes | Purge valve time: 1.5 min. Detector mode: full mass range Sample Preparation: Wetting: 1 g of dandelion root powder combined with 9 mL of water, shaken well, fortified with pesticides and QuEChERS Internal Standard Mix for GC/MS Analysis (cat.# 33267), soak for 2 hours. Extraction: 10 mL acetonitrile added then addition of Q-sep Q110 (cat.# 26213), centrifuge with Q-sep 3000 Centrifuge (cat.# 26230). cSPE: add control standard anthracene (cat.# 33264) to 1 mL extract, add magnesium sulfate to cartridge, use 6 mL Combo SPE Cartridge containing 500 mg CarboPrep 90/500 mg PSA (cat.# 26194), concentrate via evaporation. |
relativo alle ricerche nella libreria dei cromatogrammi
Consigli per la stampa! Per stampare cromatogrammi su tutta la pagina, cambiare le impostazioni di stampa nella finestra di stampa del vostro software PDF reader: 1)"adatta" o "adatta alla pagina", 2)"panorama" per cromatogrammi grandi o "ritratto" per cromatogrammi alti.
