Innovative Chromatography Products
www.restek.it
www.restek.it
Questo cromatogramma potrebbe contenere analiti che sono sinonimi dei vostri parametri di ricerca.
Semivolatiles on Rxi-5ms (Split Injection)
| Peaks | tR (min) | |
|---|---|---|
| 1. | 1,4-Dioxane-D8 (IS)  | 1.98 |
| 2. | N-Nitrosodimethylamine | 2.15 |
| 3. | Pyridine | 2.18 |
| 4. | 2-Fluorophenol (SS) | 2.87 |
| 5. | Phenol-D6 (SS) | 3.48 |
| 6. | Phenol | 3.49 |
| 7. | Aniline | 3.54 |
| 8. | bis-(2-chloroethyl)ether | 3.57 |
| 9. | 2-Chlorophenol | 3.62 |
| 10. | 1,3-Dichlorobenzene | 3.74 |
| 11. | 1,4-Dichlorobenzene-D4 (IS) | 3.76 |
| 12. | 1,4-Dichlorobenzene | 3.77 |
| 13. | Benzyl Alcohol | 3.86 |
| 14. | 1,2-Dichlorobenzene | 3.92 |
| 15. | 2-Methylphenol | 3.95 |
| 16. | Bis(2-Chloroisopropyl)ether | 3.98 |
| 17. | 4-Methylphenol | 4.06 |
| 18. | 3-Methylphenol | 4.06 |
| 19. | N-Nitrosodi-N-propylamine | 4.09 |
| 20. | Hexachloroethane | 4.17 |
| 21. | Nitrobenzene-D5 (SS) | 4.21 |
| 22. | Nitrobenzene | 4.22 |
| 23. | Isophorone | 4.41 |
| 24. | 2-Nitrophenol | 4.49 |
| 25. | 2,4-Dimethylphenol | 4.5 |
| 26. | Benzoic acid | 4.54 |
| 27. | Bis(2-chloroethoxy)methane | 4.58 |
| 28. | 2,4-Dichlorophenol | 4.67 |
| 29. | 1,2,4-Trichlorobenzene | 4.76 |
| 30. | Naphthalene-D8 (IS) | 4.79 |
| 31. | Naphthalene | 4.81 |
| 32. | 4-Chloroaniline | 4.86 |
| 33. | Hexachlorobutadiene | 4.96 |
| 34. | 4-Chloro-3-methylphenol | 5.26 |
| 35. | 2-Methylnaphthalene | 5.4 |
| 36. | 1-Methylnaphthalene | 5.49 |
| 37. | Hexachlorocyclopentadiene | 5.6 |
| 38. | 2,4,6-Trichlorophenol | 5.66 |
| 39. | 2,4,5-Trichlorophenol | 5.69 |
| 40. | 2-Fluorobiphenyl (SS) | 5.73 |
| 41. | 2-Chloronaphthalene | 5.82 |
| 42. | 2-Nitroaniline | 5.93 |
| 43. | 1,4-Dinitrobenzene | 6.02 |
| 44. | Dimethyl phthalate | 6.11 |
| 45. | 1,3-Dinitrobenzene | 6.12 |
| 46. | 2,6-Dinitrotoluene | 6.17 |
| 47. | Acenaphthylene | 6.19 |
| Peaks | tR (min) | |
|---|---|---|
| 48. | 1,2-Dinitrobenzene | 6.23 |
| 49. | 3-Nitroaniline | 6.29 |
| 50. | Acenaphthene-D10 (IS) | 6.33 |
| 51. | Acenaphthene | 6.35 |
| 52. | 2,4-Dinitrophenol | 6.38 |
| 53. | 4-Nitrophenol | 6.42 |
| 54. | Dibenzofuran | 6.49 |
| 55. | 2,4-Dinitrotoluene | 6.51 |
| 56. | 2,3,5,6-Tetrachlorophenol | 6.59 |
| 57. | 2,3,4,6-Tetrachlorophenol | 6.63 |
| 58. | Diethyl Phthalate | 6.72 |
| 59. | 4-Chlorophenyl phenyl ether | 6.79 |
| 60. | Fluorene | 6.8 |
| 61. | 4-Nitroaniline | 6.83 |
| 62. | 4,6-Dinitro-2-methylphenol | 6.87 |
| 63. | N-Nitrosodiphenylamine (as Diphenylamine) | 6.89 |
| 64. | N,N'-Diphenylhydrazine (as Azobenzene) | 6.93 |
| 65. | 2,4,6-Tribromophenol (SS) | 7.02 |
| 66. | 4-Bromophenyl phenyl ether | 7.22 |
| 67. | Hexachlorobenzene | 7.36 |
| 68. | Pentachlorophenol | 7.51 |
| 69. | Phenanthrene-D10 (IS) | 7.62 |
| 70. | Phenanthrene | 7.64 |
| 71. | Anthracene | 7.68 |
| 72. | Carbazole | 7.82 |
| 73. | di-n-Butyl phthalate | 8.16 |
| 74. | Fluoranthene | 8.73 |
| 75. | Benzidine | 8.85 |
| 76. | Pyrene-D10 (SS) | 8.95 |
| 77. | Pyrene | 8.97 |
| 78. | p-Terphenyl-D14 (SS) | 9.14 |
| 79. | 3,3'-Dimethylbenzidine | 9.74 |
| 80. | Butyl benzyl phthalate | 9.79 |
| 81. | Bis(2-ethylhexyl) adipate | 9.89 |
| 82. | 3,3'-Dichlorobenzidine | 10.6 |
| 83. | Benz[a]anthracene | 10.62 |
| 84. | Chrysene-D12 (IS) | 10.65 |
| 85. | Chrysene | 10.69 |
| 86. | Bis(2-ethylhexyl) phthalate | 10.8 |
| 87. | Di-n-octyl phthalate | 12.14 |
| 88. | Benzo[b]fluoranthene | 12.93 |
| 89. | Benzo[k]fluoranthene | 12.99 |
| 90. | Benzo[a]pyrene | 13.77 |
| 91. | Perylene-D12 (IS) | 13.93 |
| 92. | Indeno[1,2,3-cd]pyrene | 16.56 |
| 93. | Dibenz[a,h]anthracene | 16.62 |
| 94. | Benzo[ghi]perylene | 17 |
GC_EV1418
| Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) | ||||||||
| Sample | Revised SV internal standard mix (cat.# 31886) | ||||||||
| Revised B/N surrogate mix (cat.# 31888) | |||||||||
| Acid surrogate mix (4/89 SOW) (cat.# 31063) | |||||||||
| 8270 MegaMix (cat.# 31850) | |||||||||
| 8270 Benzidines mix (cat.# 31852) | |||||||||
| Benzoic acid (cat.# 31879) | |||||||||
| Diluent: | Dichloromethane | ||||||||
| Conc.: | 5.0 ng/µL (IS and SS concentrations are 20 ng/µL) | ||||||||
| Injection | |||||||||
| Inj. Vol.: | 1 µL split (split ratio 10:1) | ||||||||
| Liner: | Premium 4 mm Precision liner w/wool (cat.# 23305.5) | ||||||||
| Inj. Temp.: | 275 °C | ||||||||
| Oven | |||||||||
| Oven Temp.: | 50 °C (hold 0.5 min) to 265 °C at 28 °C/min to 285 °C at 3 °C/min to 330 °C at 20 °C/min (hold 5 min) | ||||||||
| Carrier Gas | He, constant flow | ||||||||
| Flow Rate: | 1.44 mL/min | ||||||||
| Detector | MS | ||||||||
| Mode: | Scan | ||||||||
| Scan Program: |
| ||||||||
| Transfer Line Temp.: | 280 °C | ||||||||
| Analyzer Type: | Quadrupole | ||||||||
| Source Type: | Extractor | ||||||||
| Extractor Lens: | 9mm ID | ||||||||
| Source Temp.: | 350 °C | ||||||||
| Quad Temp.: | 200 °C | ||||||||
| Electron Energy: | 70 eV | ||||||||
| Tune Type: | DFTPP | ||||||||
| Ionization Mode: | EI | ||||||||
| Instrument | Agilent 7890B GC & 5977A MSD |
relativo alle ricerche nella libreria dei cromatogrammi
Consigli per la stampa! Per stampare cromatogrammi su tutta la pagina, cambiare le impostazioni di stampa nella finestra di stampa del vostro software PDF reader: 1)"adatta" o "adatta alla pagina", 2)"panorama" per cromatogrammi grandi o "ritratto" per cromatogrammi alti.
