Innovative Chromatography Products
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Questo cromatogramma potrebbe contenere analiti che sono sinonimi dei vostri parametri di ricerca.
Semivolatiles on Rtx-5 with 5 m Integra-Guard by EPA Method 8270
| Peaks | |
|---|---|
| 1. | 1,4-Dioxane-D8 (IS)  |
| 2. | 1,4-Dioxane |
| 3. | Pyridine |
| 4. | N-Nitrosodimethylamine |
| 5. | Ethyl methacrylate |
| 6. | 2-Picoline |
| 7. | N-Nitrosomethylethylamine |
| 8. | Methyl methanesulfonate |
| 9. | 2-Fluorophenol (SS) |
| 10. | N-Nitrosodiethylamine |
| 11. | Ethyl methanesulfonate |
| 12. | Benzaldehyde |
| 13. | Phenol-D6 (SS) |
| 14. | Phenol |
| 15. | Aniline |
| 16. | Pentachloroethane |
| 17. | Bis(2-chloroethyl) ether |
| 18. | 2-Chlorophenol |
| 19. | 1,3-Dichlorobenzene |
| 20. | Dichlorobenzene-D4 (IS) |
| 21. | 1,4-Dichlorobenzene |
| 22. | Benzyl alcohol |
| 23. | 1,2-Dichlorobenzene |
| 24. | 2-Methylphenol |
| 25. | Bis(2-Chloroisopropyl)ether |
| 26. | 4-Methylphenol |
| 27. | 3-Methylphenol |
| 28. | Acetophenone |
| 29. | Nitrosopyrrolidine |
| 30. | N-Nitrosodipropylamine |
| 31. | N-Nitrosomorpholine |
| 32. | o-Toluidine |
| 33. | Hexachloroethane |
| 34. | Nitrobenzene-D5 (SS) |
| 35. | Nitrobenzene |
| 36. | N-Nitrosopiperidine |
| 37. | Isophorone |
| 38. | 2-Nitrophenol |
| 39. | 2,4-Dimethylphenol |
| 40. | Benzoic acid |
| 41. | Bis(2-chloroethoxy)methane |
| 42. | 2,4-Dichlorophenol |
| 43. | Phenyl-tert-butylamine (Phentermine) |
| 44. | 1,2,4-Trichlorobenzene |
| 45. | Naphthalene-D8 (IS) |
| 46. | Naphthalene |
| 47. | 4-Chloroaniline |
| 48. | 2,6-Dichlorophenol |
| 49. | Hexachloropropene |
| 50. | Hexachlorobutadiene |
| 51. | Caprolactam |
| 52. | N-Nitroso-N-butylamine |
| 53. | 1,4-Phenylenediamine |
| 54. | 4-Chloro-3-methylphenol |
| 55. | Isosafrole I |
| 56. | 2-Methylnaphthalene |
| 57. | 1-Methylnaphthalene |
| 58. | Isosafrole II |
| 59. | 1,2,4,5-Tetrachlorobenzene |
| 60. | Hexachlorocyclopentadiene |
| 61. | 2,4,6-Trichlorophenol |
| 62. | 2,4,5-Trichlorophenol |
| 63. | 2-Fluorobiphenyl (SS) |
| 64. | Safrole |
| 65. | Biphenyl |
| 66. | 2-Chloronaphthalene |
| 67. | 1-Chloronaphthalene |
| 68. | Diphenyl ether |
| 69. | 2-Nitroaniline |
| 70. | 1,4-Naphthoquinone |
| 71. | 1,2-Dinitrobenzene |
| 72. | Dimethyl phthalate |
| Peaks | |
|---|---|
| 73. | 1,3-Dinitrobenzene |
| 74. | 2,6-Dinitrotoluene |
| 75. | Acenaphthylene |
| 76. | 1,4-Dinitrobenzene |
| 77. | 3-Nitroaniline |
| 78. | Acenaphthene-D10 (IS) |
| 79. | Acenaphthene |
| 80. | 2,4-Dinitrophenol |
| 81. | 4-Nitrophenol |
| 82. | Dibenzofuran |
| 83. | 2,4-Dinitrotoluene |
| 84. | Pentachlorobenzene |
| 85. | 1-Naphthalamine |
| 86. | 2,3,5,6-Tetrachlorophenol |
| 87. | 2,3,4,6-Tetrachlorophenol |
| 88. | 2-Naphthalamine |
| 89. | Diethyl Phthalate |
| 90. | 4-Chlorophenyl phenyl ether |
| 91. | Fluorene |
| 92. | 2-Methyl-5-nitroaniline |
| 93. | 4-Nitroaniline |
| 94. | 4,6-Dinitro-2-methylphenol |
| 95. | N-nitrosodiphenylamine (as diphenylamine) |
| 96. | N,N'-Diphenylhydrazine (as Azobenzene) |
| 97. | 2,4,6-Tribromophenol (SS) |
| 98. | 1,3,5-Trinitrobenzene |
| 99. | Diallate |
| 100. | Phenacetin |
| 101. | 4-Bromophenyl phenyl ether |
| 102. | Atrazine |
| 103. | Hexachlorobenzene |
| 104. | 4-Aminobiphenyl |
| 105. | Propyzamide |
| 106. | Pentachlorophenol |
| 107. | Pentachloronitrobenzene |
| 108. | Phenanthrene-D10 (IS) |
| 109. | Phenanthrene |
| 110. | Anthracene |
| 111. | Carbazole |
| 112. | di-n-Butyl phthalate |
| 113. | 4-Nitroquinoline 1-oxide |
| 114. | Isodrin |
| 115. | Fluoranthene |
| 116. | Benzidine |
| 117. | Pyrene-D10 (SS) |
| 118. | Pyrene |
| 119. | Aramite I |
| 120. | p-Terphenyl-D14 (SS) |
| 121. | Aramite II |
| 122. | Dimethylaminoazobenzene |
| 123. | Chlorobenzilate |
| 124. | 3,3'-Dimethylbenzidine |
| 125. | Butyl benzyl phthalate |
| 126. | Kepone |
| 127. | Bis(2-ethylhexyl) adipate |
| 128. | 2-(Acetylamino)fluorene |
| 129. | Benz[a]anthracene |
| 130. | 3,3'-Dichlorobenzidine |
| 131. | Chrysene-D12 (IS) |
| 132. | Chrysene |
| 133. | Bis(2-ethylhexyl) phthalate |
| 134. | Di-n-octyl phthalate |
| 135. | Benzo[b]fluoranthene |
| 136. | Benzo[k]fluoranthene |
| 137. | 7,12-Dimethylbenzo[a]anthracene |
| 138. | Benzo[a]pyrene |
| 139. | Perylene-D12 (IS) |
| 140. | 3-Methylcholanthrene |
| 141. | Dibenz[a,j]acridine |
| 142. | Indeno[1,2,3-cd]pyrene |
| 143. | Dibenz[a,h]anthracene |
| 144. | Benzo[ghi]perylene |
GC_EV1357
| Column | Rtx-5 w/ 5 m Integra-Guard, 30 m, 0.25 mm ID, 0.50 µm (cat.# 10238-124) | ||||||||
| Sample | Revised SV internal standard mix (cat.# 31886) | ||||||||
| Revised B/N surrogate mix (cat.# 31888) | |||||||||
| Acid surrogate mix (4/89 SOW) (cat.# 31063) | |||||||||
| 8270 MegaMix (cat.# 31850) | |||||||||
| 8270 Benzidines mix (cat.# 31852) | |||||||||
| Benzoic acid (cat.# 31879) | |||||||||
| Appendix IX mix #1, revised (cat.# 32459) | |||||||||
| Appendix IX mix #2 (cat.# 31806) | |||||||||
| Diluent: | Dichloromethane | ||||||||
| Conc.: | 10 ng/µL (IS and SS at 20 ng/µL) | ||||||||
| Injection | |||||||||
| Inj. Vol.: | 1 µL pulsed splitless (hold 0.7 min) | ||||||||
| Liner: | Premium 4 mm single taper w/wool (cat.# 23303.5) | ||||||||
| Inj. Temp.: | 270 °C | ||||||||
| Pulse Pressure: | 30 psi (206.8kPa) | ||||||||
| Pulse Time: | 0.8 min | ||||||||
| Purge Flow: | 100 mL/min | ||||||||
| Oven | |||||||||
| Oven Temp.: | 40 °C (hold 2 min) to 90 °C at 12.5 °C/min to 246 °C at 25 °C/min to 295 °C at 3 °C/min to 325 °C at 6 °C/min (hold 3 min) | ||||||||
| Carrier Gas | He, constant flow | ||||||||
| Flow Rate: | 2.08 mL/min | ||||||||
| Detector | MS | ||||||||
| Mode: | Scan | ||||||||
| Scan Program: |
| ||||||||
| Transfer Line Temp.: | 320 °C | ||||||||
| Analyzer Type: | Quadrupole | ||||||||
| Source Type: | Inert | ||||||||
| Drawout Plate: | 9mm ID | ||||||||
| Source Temp.: | 350 °C | ||||||||
| Quad Temp.: | 180 °C | ||||||||
| Electron Energy: | 69.9 eV | ||||||||
| Solvent Delay Time: | 3.5 min | ||||||||
| Ionization Mode: | EI | ||||||||
| Instrument | Agilent 7890A GC & 5975C MSD |
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