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Questo cromatogramma potrebbe contenere analiti che sono sinonimi dei vostri parametri di ricerca.
Semivolatile Organics on Rxi-5Sil MS by U.S. EPA Method 8270
| Peaks | |
|---|---|
| 1. | 1,4-Dioxane-d8 (IS) |
| 2. | 1,4-Dioxane |
| 3. | N-Nitrosodimethylamine |
| 4. | Pyridine |
| 5. | 2-Fluorophenol (SS) |
| 6. | Phenol-d6 (SS) |
| 7. | Phenol |
| 8. | Aniline |
| 9. | Bis(2-chloroethyl) ether |
| 10. | 2-Chlorophenol |
| 11. | 1,3-Dichlorobenzene |
| 12. | 1,4-Dichlorobenzene-D4 (IS) |
| 13. | 1,4-Dichlorobenzene |
| 14. | Benzyl alcohol |
| 15. | 1,2-Dichlorobenzene |
| 16. | 2-Methylphenol |
| 17. | Bis(2-Chloroisopropyl)ether |
| 18. | 3-Methylphenol |
| 19. | 4-Methylphenol |
| 20. | N-Nitrosodi-N-propylamine |
| 21. | Hexachloroethane |
| 22. | Nitrobenzene-D5 (SS) |
| 23. | Nitrobenzene |
| 24. | Isophorone |
| 25. | 2-Nitrophenol |
| 26. | 2,4-Dimethylphenol |
| 27. | Bis(2-chloroethoxy)methane |
| 28. | Benzoic acid |
| 29. | 2,4-Dichlorophenol |
| 30. | 1,2,4-Trichlorobenzene |
| 31. | Naphthalene-D8 (IS) |
| 32. | Naphthalene |
| 33. | 4-Chloroaniline |
| 34. | Hexachlorobutadiene |
| 35. | 4-Chloro-3-methylphenol |
| 36. | 2-Methylnaphthalene |
| 37. | 1-Methylnaphthalene |
| 38. | Hexachlorocyclopentadiene |
| 39. | 2,4,6-Trichlorophenol |
| 40. | 2,4,5-Trichlorophenol |
| 41. | 2-Fluorobiphenyl (SS) |
| 42. | 2-Chloronaphthalene |
| 43. | 2-Nitroaniline |
| 44. | 1,4-Dinitrobenzene |
| 45. | Dimethyl phthalate |
| 46. | 1,3-Dinitrobenzene |
| 47. | 2,6-Dinitrotoluene |
| Peaks | |
|---|---|
| 48. | 1,2-Dinitrobenzene |
| 49. | Acenaphthylene |
| 50. | 3-Nitroaniline |
| 51. | Acenaphthene-d10 (IS) |
| 52. | Acenaphthene |
| 53. | 2,4-Dinitrophenol |
| 54. | 4-Nitrophenol |
| 55. | 2,4-Dinitrotoluene |
| 56. | Dibenzofuran |
| 57. | 2,3,5,6-Tetrachlorophenol |
| 58. | 2,3,4,6-Tetrachlorophenol |
| 59. | Diethyl phthalate |
| 60. | 4-Chlorophenyl phenyl ether |
| 61. | Fluorene |
| 62. | 4-Nitroaniline |
| 63. | 4,6-Dinitro-2-methylphenol |
| 64. | N-nitrosodiphenylamine (as diphenylamine) |
| 65. | 1,2-Diphenylhydrazine (as azobenzene) |
| 66. | 2,4,6-Tribromophenol (SS) |
| 67. | 4-Bromophenyl phenyl ether |
| 68. | Hexachlorobenzene |
| 69. | Pentachlorophenol |
| 70. | Phenanthrene-D10 (IS) |
| 71. | Phenanthrene |
| 72. | Anthracene |
| 73. | Carbazole |
| 74. | di-n-Butyl phthalate |
| 75. | Fluoranthene |
| 76. | Benzidine |
| 77. | Pyrene-d10 (SS) |
| 78. | Pyrene |
| 79. | p-Terphenyl-d14 (SS) |
| 80. | 3,3'-Dimethylbenzidine |
| 81. | Butyl benzyl phthalate |
| 82. | Bis(2-ethylhexyl) adipate |
| 83. | 3,3'-Dichlorobenzidine |
| 84. | Benz[a]anthracene |
| 85. | Chrysene-D12 (IS) |
| 86. | Bis(2-ethylhexyl)phthalate |
| 87. | Chrysene |
| 88. | Di-n-octyl phthalate |
| 89. | Benzo[b]fluoranthene |
| 90. | Benzo[k]fluoranthene |
| 91. | Benzo[a]pyrene |
| 92. | Perylene-D12 (IS) |
| 93. | Indeno[1,2,3-cd]pyrene |
| 94. | Dibenz[a,h]anthracene |
| 95. | Benzo[ghi]perylene |
GC_EV1245
| Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
| Sample | 8270 MegaMix (cat.# 31850) |
| 8270 Benzidines mix (cat.# 31852) | |
| Benzoic acid (cat.# 31879) | |
| 1,4-Dioxane (cat.# 31853) | |
| Revised B/N surrogate mix (cat.# 31888) | |
| Acid surrogate mix (4/89 SOW) (cat.# 31063) | |
| Revised SV internal standard mix (cat.# 31886) | |
| Diluent: | Dichloromethane |
| Conc.: | 8 µg/mL (IS/SS 20 μg/mL) |
| Injection | |
| Inj. Vol.: | 1 µL pulsed splitless (hold 0.59 min) |
| Liner: | Premium 4 mm single taper w/wool (cat.# 23303.5) |
| Inj. Temp.: | 270 °C |
| Pulse Pressure: | 30 psi (206.8kPa) |
| Pulse Time: | 0.64 min |
| Purge Flow: | 100 mL/min |
| Oven | |
| Oven Temp.: | 40 °C (hold 1 min) to 280 °C at 25 °C/min to 320 °C at 5 °C/min (hold 1 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1.2 mL/min |
| Linear Velocity: | 39.723 cm/sec @ 40 °C |
| Detector | MS |
| Mode: | Scan |
| Transfer Line Temp.: | 280 °C |
| Analyzer Type: | Quadrupole |
| Source Temp.: | 276 °C |
| Quad Temp.: | 150 °C |
| Solvent Delay Time: | 2.19 min |
| Tune Type: | DFTPP |
| Ionization Mode: | EI |
| Scan Range: | 35-550 amu |
| Scan Rate: | 5.36 scans/sec |
| Instrument | Agilent 7890A GC & 5975C MSD |
| Notes | 7890 Siltek treated EZ Twist Top split/splitless injection port (cat.# 22178) Gold-plated dual Vespel ring inlet seal (cat.# 21241) |
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