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Semivolatile Organics by EPA Method 8270 on Rxi-5Sil MS (30m, 0.25mm ID, 0.25 µm) w/Single Taper Liner packed with Semivolatiles Wool
| Peaks | |
|---|---|
| 1. | 1,4-Dioxane |
| 2. | N-Nitrosodimethylamine |
| 3. | Pyridine |
| 4. | 2-Fluorophenol (SS) |
| 5. | Phenol-d6 (SS) |
| 6. | Phenol |
| 7. | Aniline |
| 8. | Bis(2-chloroethyl) ether |
| 9. | 2-Chlorophenol |
| 10. | 1,3-Dichlorobenzene |
| 11. | 1,4-dichlorobenzene-d4 (IS) |
| 12. | 1,4-Dichlorobenzene |
| 13. | Benzyl alcohol |
| 14. | 1,2-Dichlorobenzene |
| 15. | 2-Methylphenol |
| 16. | Bis(2-chloroisopropyl) ether |
| 17. | 4-Methylphenol/3-Methylphenol |
| 18. | N-Nitrosodi-N-propylamine |
| 19. | Hexachloroethane |
| 20. | Nitrobenzene-d5 (SS) |
| 21. | Nitrobenzene |
| 22. | Isophorone |
| 23. | 2-Nitrophenol |
| 24. | 2,4-Dimethylphenol |
| 25. | Benzoic acid |
| 26. | Bis(2-chloroethoxy)methane |
| 27. | 2,4-Dichlorophenol |
| 28. | 1,2,4-Trichlorobenzene |
| 29. | Naphthalene-d8 (SS) |
| 30. | Naphthalene |
| 31. | 4-Chloroaniline |
| 32. | Hexachlorobutadiene |
| 33. | 4-Chloro-3-methylphenol |
| 34. | 2-Methylnaphthalene |
| 35. | 1-Methylnaphthalene |
| 36. | Hexachlorocyclopentadiene |
| 37. | 2,4,6-Trichlorophenol |
| 38. | 2,4,5-Trichlorophenol |
| 39. | 2-Fluorobiphenyl (SS) |
| 40. | 2-Chloronaphthalene |
| 41. | 2-Nitroaniline |
| 42. | 1,4-Dinitrobenzene |
| 43. | Dimethyl phthalate |
| 44. | 1,3-Dinitrobenzene |
| 45. | 2,6-Dinitrotoluene |
| 46. | 1,2-Dinitrobenzene |
| Peaks | |
|---|---|
| 47. | Acenaphthylene |
| 48. | 3-Nitroaniline |
| 49. | Acenaphthene-d10 (IS) |
| 50. | Acenaphthene |
| 51. | 2,4-Dinitrophenol |
| 52. | 4-Nitrophenol |
| 53. | 2,4-Dinitrotoluene |
| 54. | Dibenzofuran |
| 55. | 2,3,5,6-Tetrachlorophenol |
| 56. | 2,3,4,6-Tetrachlorophenol |
| 57. | Diethyl phthalate |
| 58. | 4-Chlorophenyl phenyl ether |
| 59. | Fluorene |
| 60. | 4-Nitroaniline |
| 61. | 4,6-Dinitro-2-methylphenol |
| 62. | N-Nitrosodiphenylamine (Diphenylamine) |
| 63. | 1,2-Diphenylhydrazine (as Azobenzene) |
| 64. | 2,4,6-Tribromophenol (SS) |
| 65. | 4-Bromophenyl phenyl ether |
| 66. | Hexachlorobenzene |
| 67. | Pentachlorophenol |
| 68. | Phenanthrene-d10 (IS) |
| 69. | Phenanthrene |
| 70. | Anthracene |
| 71. | Carbazole |
| 72. | di-n-Butyl phthalate |
| 73. | Fluoranthene |
| 74. | Benzidine |
| 75. | Pyrene-d10 (SS) |
| 76. | Pyrene |
| 77. | p-Terphenyl-d14 (SS) |
| 78. | 3,3'-Dimethylbenzidine |
| 79. | Butyl benzyl phthalate |
| 80. | Bis(2-ethylhexyl) adipate |
| 81. | 3,3'-Dichlorobenzidine |
| 82. | Benz[a]anthracene |
| 83. | Bis(2-ethylhexyl)phthalate |
| 84. | Chrysene-d12 (IS) |
| 85. | Chrysene |
| 86. | Di-n-octyl phthalate |
| 87. | Benzo[b]fluoranthene |
| 88. | Benzo[k]fluoranthene |
| 89. | Benzo[a]pyrene |
| 90. | Perylene-d12 (IS) |
| 91. | Dibenz[a,h]anthracene |
| 92. | Indeno[1,2,3-cd]pyrene |
| 93. | Benzo[ghi]perylene |
C = Toluene
GC_EV01129
| Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
| Sample | 8270 MegaMix (cat.# 31850) |
| Benzoic acid (cat.# 31879) | |
| 8270 Benzidines Mix (cat.# 31852) | |
| Acid Surrogate Mix (4/89 SOW) (cat.# 31025) | |
| Revised B/N Surrogate Mix (cat.# 31887) | |
| 1,4-dioxane (cat.# 31853) | |
| SV Internal Standard Mix (cat.# 31206) | |
| Diluent: | methylene chloride |
| Conc.: | 10 ng on-column |
| Injection | |
| Inj. Vol.: | 1.0 µL pulsed splitless (hold 0.25 min) |
| Liner: | Singel Taper Splitless (4mm) w/Application-Specific Wool (cat.# 20798-231.1) |
| Inj. Temp.: | 250 °C |
| Pulse Pressure: | 25 psi (172.4kPa) |
| Pulse Time: | 0.3 min |
| Purge Flow: | 60 mL/min |
| Oven | |
| Oven Temp.: | 40 °C (hold 1 min) to 280 °C at 25 °C/min to 320 °C at 5 °C/min (hold 1 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1.2 mL/min |
| Detector | MS |
| Mode: | Scan |
| Transfer Line Temp.: | 280 °C |
| Analyzer Type: | Quadrupole |
| Source Temp.: | 250 °C |
| Tune Type: | DFTPP |
| Ionization Mode: | EI |
| Scan Range: | 35-550 amu |
| Instrument | Agilent 7890A GC & 5975C MSD |
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