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Organochlorine Pesticides by EPA Method 8081A on Rtx-440 (dual column w/ Rtx-CLPesticides2)

Column | Rtx-440, 30 m, 0.32 mm ID, 0.50 µm (cat.# 12939) |
Sample | Organochlorine pesticide mix AB #2, 8-80 µg/mL in ethyl acetate (cat.# 32292) |
Chlorobenzilate, 1,000 µg/mL in methanol (cat.# 32211) | |
Hexachlorobenzene, 1,000 µg/mL in acetone (cat.# 32231) | |
Hexachlorocyclopentadiene, 1,000 µg/mL in methanol (cat.# 32232) | |
2,4'-DDD, 1,000 µg/mL in methanol (cat.# 32098) | |
2,4'-DDE, 1,000 µg/mL in methanol (cat.# 32099) | |
2,4'-DDT, 1,000 µg/mL in methanol (cat.# 32200) | |
2,4,5,6-Tetrachloro-m-xylene, 200 µg/mL in acetone (cat.# 32027) | |
Decachlorobiphenyl (BZ #209), 200 µg/mL in acetone (cat.# 32029) | |
Diallate (cis & trans), 1,000 µg/mL in hexane (cat.# custom) | |
Isodrin, 1,000 µg/mL in hexane (cat.# custom) | |
Kepone, 1,000 µg/mL in hexane (cat.# custom) | |
Mirex, 1,000 µg/mL in hexane (cat.# custom) | |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.75 min) |
Liner: | Siltek single taper (cat.# 20961-214.1) |
Inj. Temp.: | 275 °C |
Oven | |
Oven Temp.: | 140 °C (hold 1 min) to 240 °C at 30 °C/min (hold 2 min) to 330 °C at 30 °C/min (hold 4 min) |
Carrier Gas | H2, constant pressure |
Linear Velocity: | 51 cm/sec @ 140 °C |
Detector | ECD @ 330 °C |
Instrument | Shimadzu 2010 GC |
Notes | Rtx-CLPesticides2 analysis shown in chromatogram GC_EV00797. |
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