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Organophosphorus Pesticides (European) on Rtx-CLPesticides

Column | Rtx-CLPesticides, 30 m, 0.25 mm ID, 0.25 µm (cat.# 11123) |
Sample | Custom European Mix |
1-Bromo-2-nitrobenzene (cat.# 32279) | |
4-Chloro-3-nitrobenzotrifluoride (cat.# 32282) | |
Tributylphosphate (cat.# 32280) | |
Triphenylphosphate (cat.# 32281) | |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.4 min) |
Liner: | Double Gooseneck Splitless (4mm) (cat.# 20785) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 80 °C (hold 1.0 min) to 150 °C at 7 °C/min to 280 °C at 15 °C/min (hold 7 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 0.75 mL/min |
Linear Velocity: | 28 cm/sec |
Dead Time: | 1.82 min @ 80 °C |
Detector | MS |
Mode: | Scan |
Transfer Line Temp.: | 280 °C |
Solvent Delay Time: | 5 min |
Tune Type: | PFTBA |
Ionization Mode: | EI |
Scan Range: | 35-400 amu |
Instrument | Agilent 5971A GC/MS |
Notes | Carrier gas @ 6 psi head pressure |
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