Innovative Chromatography Products
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www.restek.it
Derivatized Cannabinoids (5 μg/mL) on Rxi-5Sil MS
| Peaks | |
|---|---|
| 1. | Cannabidiol |
| 2. | delta 9 THC |
| Peaks | |
|---|---|
| 3. | Cannabinol |
| 4. | THC-COOH; THCA |
GC_CF1145
| Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
| Sample | |
| Diluent: | Ethyl acetate |
| Conc.: | 5 µg/mL TMS derivatives |
| Injection | |
| Inj. Vol.: | 1 µL splitless (hold 1 min) |
| Liner: | 3.5 mm taper splitless w/wool (cat.# 22286-200.1) |
| Inj. Temp.: | 250 °C |
| Purge Flow: | 21.4 mL/min |
| Oven | |
| Oven Temp.: | 150 °C to 330 °C at 15 °C/min (hold 3 min) |
| Carrier Gas | He, constant linear velocity |
| Linear Velocity: | 40 cm/sec, 13.8 psi, 95.1 kPa @ 150 °C |
| Detector | MS |
| Mode: | Scan |
| Transfer Line Temp.: | 280 °C |
| Analyzer Type: | Quadrupole |
| Source Temp.: | 200 °C |
| Electron Energy: | 70 eV |
| Solvent Delay Time: | 4 min |
| Tune Type: | PFTBA |
| Ionization Mode: | EI |
| Scan Range: | 200-500 amu |
| Scan Rate: | 5 scans/sec |
| Instrument | Shimadzu 2010 GC & QP2010+ MS |
relativo alle ricerche nella libreria dei cromatogrammi
Consigli per la stampa! Per stampare cromatogrammi su tutta la pagina, cambiare le impostazioni di stampa nella finestra di stampa del vostro software PDF reader: 1)"adatta" o "adatta alla pagina", 2)"panorama" per cromatogrammi grandi o "ritratto" per cromatogrammi alti.
