Innovative Chromatography Products
www.restek.it
www.restek.it
Basic Drugs (Underivatized) on Rxi-5MS
| Peaks | |
|---|---|
| 1. | Amphetamine |
| 2. | Methamphetamine |
| 3. | Nicotine |
| 4. | Cotinine |
| 5. | Caffeine |
| 6. | Benzphetamine |
| Peaks | |
|---|---|
| 7. | Ketamine |
| 8. | Phencyclidine |
| 9. | Methadone |
| 10. | Cocaine |
| 11. | Scopolamine |
| 12. | Codeine |
| 13. | Alprazolam |
GC_CF00855
| Column | Rxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423) |
| Sample | basic drugs |
| Diluent: | methanol |
| Conc.: | 10 µg/mL each drug, 1 ng on column |
| Injection | |
| Inj. Vol.: | 1.0 µL split (split ratio 10:1) |
| Liner: | Gooseneck Splitless (4mm) w/Wool Siltek Liner |
| Inj. Temp.: | 250 °C |
| Oven | |
| Oven Temp.: | 100 °C to 300 °C at 20 °C/min (hold 5 min) |
| Carrier Gas | He, constant flow |
| Flow Rate: | 1 mL/min |
| Detector | MS |
| Mode: | Scan |
| Transfer Line Temp.: | 300 °C |
| Ionization Mode: | EI |
| Scan Range: | 35-550 amu |
| Notes | Gooseneck Splitless (4mm) w/Wool Siltek Liner, recommend catalog number 20798. |
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