Explosives by EPA 8330B on Ultra C8 with Trident Direct Guard Column

Peaks
1.HMX
2.RDX
3.1,3,5-Trinitrobenzene
4.1,4-Dinitrobenzene (SS)
5.1,3-Dinitrobenzene
6.Nitrobenzene
7.3,5-Dinitroaniline
8.Tetryl
9.2,4,6-Trinitrotoluene
Peaks
10.Nitroglycerin
11.2,4-Dinitrotoluene
12.4-Amino-2,6-dinitrotoluene
13.2,6-Dinitrotoluene
14.2-Amino-4,6-dinitrotoluene
15.2-Nitrotoluene
16.4-Nitrotoluene
17.3-Nitrotoluene
18.PETN
image
LC_EV0526
ColumnUltra C8 (cat.# 9103565)
Dimensions:150 mm x 4.6 mm ID
Particle Size:5 µm
Pore Size:100 Å
Temp.:30 °C
Sample8330B Nitroaromatics and nitramine mix (cat.# 33204)
1,4-Dinitrobenzene (cat.# 33205)
Diluent:Deionized water
Conc.:20 µg/mL
Inj. Vol.:10 µL
Mobile PhaseWater:methanol (52:48)
Flow:1.2 mL/min
DetectorUV/Vis @ 210/254 nm
InstrumentShimadzu UFLCXR
NotesTrident direct 10 mm in-line guard cartridge holder (cat.# 25083)
Ultra C8 10 mm x 4 mm guard cartridge (cat.# 910350210)

This is the recommended primary column for a 2 column analysis. See LC_EV0527 for the confirmation column.
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