GC Multiresidue Pesticide Standard #2-OCP on Rxi-5ms by GC-MS

PeakstR (min)
1.Chloroneb10.10
2.Pentachlorobenzene10.31
3.alpha-BHC12.70
4.Hexachlorobenzene12.90
5.Pentachloroanisole13.02
6.beta-BHC13.36
7.gamma-BHC (Lindane)13.52
8.delta-BHC14.09
9.Endosulfan ether14.55
10.Heptachlor15.25
11.Pentachlorothioanisole15.83
12.Aldrin16.06
13.4,4'-Dichlorobenzophenone16.26
14.Fenson16.45
15.Isodrin16.72
16.Heptachlor epoxide (Isomer B)16.97
17.Chlorbenside17.37
18.trans-Chlordane17.51
19.2,4'-DDE17.62
20.Endosulfan I17.79
PeakstR (min)
21.cis-Chlordane17.85
22.trans-Nonachlor17.96
23.Chlorfenson (Ovex)17.97
24.4,4'-DDE18.31
25.Dieldrin18.37
26.2,4'-DDD18.50
27.Endrin18.85
28.Ethylan (Perthane)18.86
29.Endosulfan II19.04
30.4,4'-DDD19.23
31.2,4'-DDT19.31
32.cis-Nonachlor19.33
33.Endrin aldehyde19.45
34.4,4'-Methoxychlor olefin19.84
35.Endosulfan sulfate19.97
36.4,4'-DDT20.04
37.2,4'-Methoxychlor20.27
38.Endrin ketone20.97
39.Tetradifon21.68
40.Mirex22.16
image
GC_FS0601
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleGC multiresidue pesticide standard #2-OCP (cat.# 32564)
Diluent:Toluene
Conc.:100 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Premium 4.0 mm ID Precision inlet liner w/wool (cat.# 23305.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.4 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
1555-5507
Transfer Line Temp.:290 °C
Analyzer Type:Quadrupole
Source Temp.:325 °C
Electron Energy:70 eV
Solvent Delay Time:5 min
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
NotesReconstructed chromatogram from select ions.
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