Organochlorine Pesticides US EPA Method 8081 on Rtx-XLB

Peaks
1.2,4,5,6-Tetrachloro-m-xylene (ss)
2.α-BHC
3.γ-BHC
4.β-BHC
5.δ-BHC
6.Heptachlor
7.Aldrin
8.Heptachlor epoxide
9.γ-Chlordane
10.α-Chlordane
11.Endosulfan I
Peaks
12.4,4'-DDE
13.Dieldrin
14.Endrin
15.4,4'-DDD
16.Endosulfan II
17.Endrin aldehyde
18.4,4'-DDT
19.Endosulfan sulfate
20.Methoxychlor
21.Endrin ketone
22.Decachlorobiphenyl (ss)
image
ColumnRtx-XLB, 30 m, .32 mm ID, .5 µm (cat.# 12839)
SampleOrganochlorine Pesticide Mix AB #2 (cat.# 32292)
2,4,5,6-tetrachloro-«M,67[m (meta)]»-xylene (cat.# 32027)
decachlorobiphenyl (BZ #209) (cat.# 32029)
Conc.: Organochlorine Pesticide Mix AB (cat.# 32292) 80/160ppb in hexane 2,4,5,6-tetrachloro- m-xylene (cat.# 32027) surrogate, 80ppb decachlorobiphenyl (cat.# 32029) surrogate, 160ppb
Injection
Inj. Vol.:1.0 µL splitless (hold 0.75 min)
Liner:Drilled Uniliner (hole near top) (cat.# 21055)
Inj. Temp.:220 °C
Oven
Oven Temp.:120 °C (hold 0.5 min) to 260 °C at 29 °C/min (hold 2.5 min) to 330 °C at 28 °C/min (hold 3 min)
Carrier GasH2, constant pressure
Linear Velocity:60 cm/sec @ 120 °C
DetectorECD @ 320 °C
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