Organochlorine Pesticides US EPA Method 8081 on Rtx-CLPesticides

Peaks
1.2,4,5,6-Tetrachloro-m-xylene
2.α-BHC
3.γ-BHC
4.β-BHC
5.δ-BHC
6.Heptachlor
7.Aldrin
8.Heptachlor epoxide
9.γ-Chlordane
10.α-Chlordane
11.4,4'-DDE
Peaks
12.Endosulfan I
13.Dieldrin
14.Endrin
15.4,4'-DDD
16.Endosulfan II
17.4,4'-DDT
18.Endrin aldehyde
19.Methoxychlor
20.Endosulfan sulfate
21.Endrin ketone
22.Decachlorobiphenyl
image
GC_EV00636
ColumnsRtx-CLPesticides 30 m, 0.32 mm ID, 0.50 µm (cat.# 11139)
and Rtx-CLPesticides2 30 m, 0.32 mm ID, 0.25 µm (cat.# 11324)
SampleOrganochlorine Pesticide Mix AB #2 (cat.# 32292)
Pesticide Surrogate Mix, EPA 8080, 8081 (cat.# 32000)
Conc.: 20–400µg/mL Organochlorine Pesticide Mix AB #2 (cat.# 32292) in hexane:toluene (1:1) 200µg/mL Pesticide Surrogate Mix (cat.#32000 ) in acetone
Injection
Inj. Vol.:1.0 µL Direct
Liner:Drilled Uniliner (hole near top) (cat.# 21054)
Inj. Temp.:225 °C
Oven
Oven Temp.:110 °C (hold 1 min) to 245 °C at 20 °C/min to 310 °C (hold 1 min)
Carrier GasHe, constant pressure
Linear Velocity:53 cm/sec @ 110 °C
DetectorECD @ 330 °C
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